MaTecK GmbH
   
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Last Update
1st July 2007
 
Metal single crystals

Production of metallic single crystals is carried out in most modern equipment with highest quality requirements. For crystal growth using the Bridgman-, Czochralski- and zone melting techniques only highest purity starting materials are used. The following metallic single crystals are normally available from the shelf:

  !! New !!    
 Metal single crystal Crystal geometry
 Purity Info
 Aluminium - Al click for more details  6N
 Antimony - Sb click for more details  6N2
 Bismut - Bi click for more details  5N
 Cadmium - Cd click for more details  5N
 Chromium - Cr click for more details  5N
 Cobalt - Co click for more details  4N
 Copper - Cu click for more details  5N
 Dysprosium - Dy click for more details  3N5
 Gadolinium - Gd click for more details  4N
 Germanium - Ge click for more details  6N
 Gold - Au click for more details  5N
 Hafnium - Hf click for more details  4N ex Zr
 Holmium - Ho click for more details  3N5
 Indium - In click for more details  6N
 Iridium - Ir click for more details  4N
 Iron - Fe click for more details  4N
 Lead - Pb click for more details  5N
 Lithium - Li click for more details  2N8
 Magnesium - Mg click for more details  5N
 Molybdenum - Mo click for more details  4N
 Nickel - Ni click for more details  4N
 Niobium - Nb click for more details  4N
 Palladium - Pd click for more details  5N
 Platinum - Pt click for more details  4N
 Rhenium - Re click for more details  4N
 Rhodium - Rh click for more details  4N
 Ruthenium Ru click for more details  4N
 Silicon - Si click for more details  5N
 Silver - Ag click for more details  5N
 Tantalum - Ta click for more details  4N
 Tellurium - Te click for more details  6N
 Tin - Sn click for more details  6N
 Titanium* - Ti click for more details  4N
 Tungsten - W click for more details  5N
 Vanadium - V click for more details  4N
 Yttrium - Y click for more details  3N5
 Zinc - Zn click for more details  6N
 Zirconium - Zr click for more details  4N ex Hf*

* crystal size limited to a few millimeters

Alloy crystals such as Cu2Ce, CuAu, Cu3Au, Cu3Pd, Cu3Pt, Cu75Mn25, CuNi,CoAl, CoGa, FeAl, FeCr, Fe85Cr15, Fe64Ni36, Fe80Ni20, Nb90W10, NiAl ,Ni3Al, Ni3Al (+Fe), NiFe, Pd97Ni3, Pt7Ni, Pt75Ni25, Pt48Ni52, Pt3Cu, PtCo3, Pt3Cr, Pt10Pd90, PtPd, Pt90Pd10, PtRh, Pt80Rh20, Pt90Rh10,Pt95Rh5, TbCu2, V3Si, W99Re1 are partially on stock as well. Further unlisted alloy crystals can be grown according to specifications of the customer.

Orientation and Polishing
The standard orientations offered for the above crystals are for the cubic system (001), (110) and (111) for hexagonal crystals (0001), (10-10) und (11-20). Other orientations such as (117), (221) or (112) may also be produced, of course. The standard accuracy of the orientation of cut crystals is within < 2°. By surface polishing an accuracy of < 0,1° is achievable. Polishing of the different crystals is performed very gently and where possible done chemomechanically. A surface roughness of better than < 0,03µm is obtained. Based on such a polish an atomically smooth surface may be prepared with a few sputter- and heating cycles or by flame annealing. (Recipes for the surface preparation in UHV are available on request). Given an orientation accuracy of < 0,1° terrace widths of several thousand Angstrom are achieved.

Picture: Metal single crystals

Crystal geometry
Metallic single crystals are usually pulled in form of rods. Depending on the metal the rod diameter can be set to values between several millimeters to 100 mm. These rods can be supplied either as raw crystals without further shaping or cut to discs. A standard disc thickness is 1mm. Thicker or thinner discs are supplied on request.
The crystal geometry is shaped according to specifications of the customer by spark erosion. Special geometries, grooves, holes and reference faces (for instance, to indicate a second orientation) are possible without problems. Below a few common examples are listed .

Please click on the drawing to choose your geometry. For crystal offers or orders just fill in your desired measures and send us these drawings. - If your design is not included, please fax us your drawing or hand sketch.

"Hat form" with indication of second orientation :
Picture: Hat form

circular groove, reference face to mark a second orientation and hole for a thermocouple :
Picture: circular groove

Holes for keeping crystal in place :
Picture: holes



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